DEMETER - Narodowe Centrum Promieniowania Synchrotronowego SOLARIS

Beamlines

DEMETER

DEMETER beamline is specialized research installation using variable polarization radiation, the source of which is the EPU undulator (elliptically polarizing undulator).

The concept of the beamline DEMETER (Dual Microscopy and Electron Spectroscopy Beamline) assumes the coexistence of two measurement branches, in which the research end stations is the PEEM microscope (photoemission electron microscope) together with the addition of an electron column creating a Low Energy Electron Microscope (LEEM), all together constituting the SPELEEM system (Spectroscopic PhotoEmission and Low Energy Electron Microscope) and STXM (scanning transmission X-ray microscope).   

The PEEM/LEEM end station with standard equipment will allow for the creation and modification of research systems and imaging of their surfaces in a wide range of temperatures and with high resolution. The main advantage of the method is the ability to select the energy of excitations and the possibility of tuning to the characteristic edge of the absorption. The PEEM station is designed for real-time imaging of surface nanostructures at the mesoscale in the temperature range from -160 °C to 1200 °C. The microscope can measure flat samples prepared both ex-situ and in-situ. The available temperature range using liquid nitrogen is -100 °C and using liquid helium is -160 °C. 

A special advantage of the microscope is the possibility of simultaneous imaging with chemical and magnetic contrast using X-ray magnetic circular and linear dichroism (XMCD and XMLD) on the corresponding absorption edges of ferromagnetic and antiferromagnetic materials.

The parent institution for the PEEM end station is the Jerzy Haber Institute of Catalysis and Surface Chemistry of the Polish Academy of Sciences (ICSC PAS). Thanks to the collaboration of SOLARIS with the Jerzy Haber Institute of Catalysis and Surface Chemistry of the Polish Academy of Sciences and the AGH University of Science and Technology in Kraków (AGH-UST) on March 2, 2016, an appropriate agreement was signed (event information) under which the PEEM end station is made available to Users in the synchrotron facility. As part of the cooperation, the infrastructure for the end station is maintained and developed, and the support of the microscope operators during the measurements is provided. 

The STXM end-station will provide chemical analysis at the nanoscale through the combination of X-ray absorption spectrometry and microscopy. 

Potential application of the beamline:

  • Magnetic order research 
  • Domain structure research 
  • Imaging of the chemical composition 
  • Biomolecular spectroscopy 
  • Fluorescence detection. 

The ICSC PAS and AGH-UST invite users who have been granted beam time to cooperate: 

Beamline parameters

Parameters Value
Source Elliptically polarizing undulator (EPU)
Available energy range  100–2000 eV (horizontal linear polarization)
Energy resolution ΔE/E 1-10 x 10-4
Beam size at sample (H x V)  PEEM: 200 (h) x 40 (v) μm2
STXM: diameter 30 nm (min) – 300 μm (max)
Photon flux at sample 109-1012 [ph/s]
Polarization circular (left- and right-handed), elliptical, linear (horizontal and vertical)
End stations PEEM, STXM
End station
DEMETER-PEEM

PEEM operator support is available as follows:

Working days: 9:00 AM – 11:00 PM

Saturdays: 9:00 AM – 5:00 PM

Sundays: For experienced users able to operate the microscope autonomously, measurements may be conducted with prior contact with your local contact and the user office. The PEEM operator is not available on Sundays, only on call for emergency situations.

 

Available:
Imaging techniques: X-PEEM, XAS-PEEM, XMCD-PEEM, XMLD-PEEM, LEEM;
Microspot diffraction and spectroscopy techniques: μ-XAS, μ-LEED, μ-ARPES

End station
DEMETER-STXM

Microscope operator support is provided during standard working days from 9:00 AM to 5:00 PM. Outside these hours, including evenings and weekends, the operator is on call. On Saturdays, support is available on call, while on Sundays on-call support is limited to emergency issues only. 

 

Available:
- imaging in transmission: multiplier tube (PMT) and avalanche photodiode (APD) detection

 

Available at expert mode:
- Silicon drift detector (SDD) - Amptek X123 Fast SSD detector with sensitivity for photons with energy above about 200 eV
- electrochemical cell system (for liquids and gases)

 

During implementation (not available):
- measurements using a controlled external magnetic field
- ability to control the measurement geometry (angle of incidence)
- electrochemical cell system for suspensions or solids
- environmental cell system with heating option (RT-475 K)